Phenylaminopropane, And 3,4,Methyl-Ene-Dioxymeth-Phenylaminopropane Essay, Research Paper
Re: DETAILED METHODS for NON-CHEMISTS
METHamphetamine PRECURSS CLEANING/wkUP
Extractomania……..by Ozbee friends……….edited by Placebo
INDEX:
1: Equipment
2: Ingredients
3: Method
step 1:
step 2:
step 3:
step 4:
step 5:
step 6:
4: Acid/Base
5: HCl-Gassing
6: Notes
1: Equipment
* Various jars, glass vessels, beakers etc
* PH paper, electronic PH tester
* Filter paper coffeee filters
* A strainer that will fit your filters nicely,
so that you get better surface area then a funnel
* Hair dryer, heat lamps
* Hot plate, no open flames, only heat elements
* Seperaty funnel, similar, tube to siphon
2: Ingredients
-Pills containing psuedo-ephedrine HCl ephedrine HCl.
-NaOH/Sodium Hydroxide/caustic soda/strong base/lye.
-Epsom salts that have been baked in oven 200c f an hour to dry.
-Methanol
-Acetone
-Toluene
-Distillated water
3: Method
***e*** :
If pills have red coating, put in jar, with acetone, shake until red coating is dissolved then continue as
below.
Step 1: First, put your pills in a jar.
Add methanol about double the volume of the pills.
Cap the jar shake till they break apart.
Leave to sit f a few hours shaking every 1/2 hour.
Let settle into 2 nice layers then siphon decant off top layer.
No need to get it all as we will do this 2 me times to be sure get all that pseudo.
step 2: Once you have done it 3 times have the 3 lots of methanol from above, put them together
put in freezer.
You want to get it real cold, near freezing then filter it thru a very fine filter, this may take some time if
you don’t have a vacuum filtration setup but thats ok, we aint in a hurry.
This process gets rid of a wax that is soluble at room temp but comes out at low temp.
step 3:***e*** : This step is necessary only speeds things up.
After the chilled filter, we will reduce the volume of methanol/pseudo solution.
So, with good ventilation a fan blowing over pot, just reduce the volume of methanol, but till you
see crystals anything. Just reduce it to a manageable amount, we just want a saturated solution, you’ll
ice it thicken a bit. Stop, take it off.
step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirr glass table f
fast evapation, you could just leave it laying around a couple of days let nature take its course,
it does make pretty crystals. Scrape all your crystals up when they are dry put into aher clean pyrex
vessel.
step 5: Now pour Toluene, about double your psuedo volume **dry/anhydrous**use your epsoms!** over
your powdered psuedo, heat till just befe boiling with your fan blowing over it.
Boil f 5 mins then filter. Repeat this with fresh toluene until when you boil toluene it stays clear. To be
sure of toluene doing its job, after filtering, add water to toluene befe discarding you’ll see the *censored*
come out.
step 6: Next you can do an acetone wash, by putting your psuedo some acetone in a jar, shake
filter. Dry pseudo you should have *censored*in clean pseudo HCl……
This procedure, rids the pills of:
MCC
waxes
polymers
lactose
most *censored*!
BUT, povidone! Me on that later.
You may choose to react your psuedo now.
Or do an A/B acid/base extraction, basicly turn it into a freebase, oil.
keep in mind..If you do an A/B now, you may lose some psuedo to the povidone.
So what are the choices? well, povidone is known to go thru Hi/RP, no problem, but must be steam distilled
out after. which is a good thing coz you got no seperations emulsions the cleanest meth around.
Povidone is bad because povidone is known to absb hold amines. It depends on what reaction your
doing!
4: A/B: Ok, get your nice dry white powder add about equal part water.
Now make up a 20% NaOH solution 4 parts DH2O:1 part NaOH.
Add Toluene to water/pseudo solution about equal to water volume.
Yes, toluene first, it gives the pseudo somewhere to go instead of being burned by the base which can break
it up turn it into aziradines!toxic!
Add NaOH solution to water/pseudo/toluene solution till PH 13, remember to test PH of water toluene!
Now shake the jar up very well let settle into layers.
Seperate toluene layer. Repeat this process 3 times combine all your toluene.
You can wash the toluene/pseudo freebase with water now, if you like, seperate again.
Now you can either, evapate toluene f freebase crystals, you need to turn the freebase into a Hcl salt
again.
So you can add fresh DH2O about 2mL f each gram of pseudo to your toluene drop HCl acid slowly
with shaking each time into the toluene. Check pH all the time stop just befe neutral. Shake again,
recheck, this is very tricky takes patience.
Now seperate the water from the toluene.
Now you can evapate your water to get your pure pseudo HCl.
You can repeat this aher 1 2 times get a little me.
5: Gassing,
Gassing makes things easier coz you just gas it, filter there’r your crystals, but it is tricky to get the
hang of it Hydrogen Chlide is dangerous! It will burn your *censored*in lungs instantly if inhaled too much of it!
You need to pipe HCl gas into your jar full of toluene pseudo freebase, but the gas your toluene must
be dry : no water, everytime the gas fms crystals it will be reabsbed by the miniscule amounts of
water.
If you don’t know how to extract, you shouldn’t play with gas yet.
If you know how to gas then read on…
So, you need to dry your toluene/pfed solution with pre-baked epsom salts to absb the water, then
filter them out. Then gas your solution you will see a snow stm befe your very eyes.
Then just filter dry crystals.
But still may contain povidone.
Post merely f infmational purposes. I haven’t done anything illegal n should you.
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METHamphetamine synthesis
I.—-Placebo’s compilation of “the Cure” by Ozbee clean-up of sudafed other ephedrine pills
various RP/I2red phosphous / elemental iodine, pure, crystals methods.
placebo
Hive Researcher
07-04-00 11:04
Go to whoah!
Ok, this is a compilation of many peoples’ methods.
I believe this to be the best, simplest, fastest, cleanest method f producing meth-amphetamine,
in the highest yields possible f RP/I2/E reaction.
Remember, each every step gives small losses, this method has the least steps!
It is a culmination of effts by wlock, CHEMMAN, maybe a few tiny touches by me.
I re-iterate, I don’t want any congratulations except f the write-up itself.
You will need these things, no substitutions allowed.
If you can’t get this *censored*, you ain’t ready to make the best Go-Go in town.
This is a refinement of all methods, the next step up from Push Pull, but nobody should be discouraged
from attempting this, as you will probably find it easier.
pH paper isn’t even necessary.
This post is one method from Go to whoah.
This post has to be followed from Go to whoah.
Otherwise you can run into trouble, as povidone is removed in this extraction.
It will be removed at the end. Each step was chosen to complement the next.
Underst?
Read on…..
Index:
1: Equipment
2: Reagents
3: Extraction of pfed
4: Reaction
5: Steam distillation
6: Crystallisation
Equipment:
Various jars
2L pyrex vessel
2L 2 neck round flat bottom flask
1 condenser, I recommend a coil condenser but a Liebig will suffice.
1 sloping splashhead better, a steam distillation sloping splashhead.
A steam pressure cooker, that has a release-valve on top.
Hotplate, electric of course.
Filter paper, Buchner vacuum would be nice too.
Thermometer.
1 Glass stopper.
Lengths of clear pvc tubing.
Pot with vegetable oil, which can fit your reaction vessel.
Reagents:
Iodine crystals.
Red Phosphous.
Pseudo-ephedrine, ephedrine.
Methanol.
Toluene.
Acetone.
NaOH.
All must be clean anhydrous.
Ice.
Extraction of pfed:
This method will deal with the HCl salt of pfed, a streamlined version of “the Cure”.
All pills are dumped into a large jar double of this pills-volume in the fm of methanol poured on top.
This is stirred vigourously let st to settle thereafter, in the fridge seems to speed it up.
After the top methanol layer has cleared it is carefully decanted off.
This procedure is repeated 3 times.
All methanol pulls are put together the methanol boiled off on a hotplate.
As methanol gets down to the last little bit, it is taken off the heat.
Then a ption of acetone, twice your remaining liquid is dropped in.
This fces the pfed crystals to crash out.
Then the remaining liquid is carefully evaped off.
washes:
Now you have your crude/dirty pfed HCl.
Next we will be doing successive toluene washes.
Put your pfed crystals in a pyrex heat proof glass.
Now add toluene to a safe level that can be lightly boiled on the hotplate.
After about 5 mins boiling with stirring, take off the heat let it settle a minute.
Now carefully pour off toluene into a filter to catch any remnants of pfed that may follow.
Now if you get the toluene that has our contaminants in it add some water, you will see the crap, crash
from the toluene into the water.
This is the crap that came thru with the methanol pull.
So as we continue to do multiple toluene washes, we will continue to test the toluene after pouring it off, to
see how we are progressing with the cleanup.
when we have reached a point where no crap comes out of the toluene, with the addition of water, then we
are ready to try acetone.
Usually about 3 boils in toluene, but of course it depends how much you’r using.
So, as befe we will add a ption of acetone boil lightly.
Now when we pour off the acetone, we will add a tiny amount of water some NaOH.
This is our final test, when you do this no crap falls out of acetone you are ready.
This will be the cleanest pfed you have ever seen, guarenteed!
, yields should be *90% if you’r carefull! 95% is good.
Reaction :
Smallest reaction to be attempted, especially by newbees, is 1 oz of pfed, so that even taking into account
sloppiness, lack of experience losses along the way, you should get some product.
Ratios of reagents are: 3:3:1 1:1:1/3 , ie.E:I:RP aka, equal amounts of Iodine pfed, a one third
amount of RP.
This is calculated on a weight basis, can be scaled up down as necessary, e.g.60gmE/60gmI2/20gmRP
120gmE/120gmI2/40gmRP etc etc.
First prepare yourself an icebath. Yes, icecubes water in a sink bucket.
Now, many will say you should add this first that first.
well, after much reading of different peoples methods, I say….
Chuck the whole shebang in together, while your flask is on ice, lift swirl ingredients together, while
maintaing on ice.
Put your condenser on top start water running thru, from bottom to top.
Now, the idea is to get the reaction going in the most controlled way possible, you want to let the reagents
react in the container vessel fixed in the icebath, if at all.
Then move vessel from icebath to room temp.
If things look like they’re going too fast, put back in ice bath, you want to keep the reaction going but only
at a nice slow, controlled pace.
This is also necessary to control vapour in the condenser!
Thick dis-coled smoke is bad, plumes of smoke will escape from condenser.
Let things progress at a nice slow pace, as things slow too much, you can start applying heat.
So prepare an oilbath bring to about 50 C, if there is no me action in your vessel.
You can move it to the oilbath, the same goes f it as befe, when things slow down.
Adjust heat up, to say 100 C then 150 C f one hour, to make sure reaction has completed.
The whole time you should be watching to keep a nice reflux going, too much vapour is escaping
from condenser.
Now remove from heat disconnect condenser, add ice water to quench reaction.
The reason f ice water is to calm the reaction down when NaOH is added.
Its up to you if you want to filter out RP leave it in untill the end.
I would leave it, it will be washed nicely by next process be easier to filter.
Now add lots of NaOH to bring reaction mix to + 14 pH.
You can over-basify, as meth won’t be destroyed, its a tough MF!
Steam Distillation :
Now you need to set up your glassware f steam distillation.
Attach the steam distillation sloping splashhead to top hole of flask, attach plastic hose to steam inlet
the other end on the release valve of the pressure cooker that is full of water.
Attach condenser on the end of splashhead, rig the whole up so it stays up.
Place a jar at the end of condenser to catch our distillate.
You want to heat both the pressure cooker, the reaction flask.
Sit back get ready f one of the most beautiful sights smells.
The meth freebase that is sitting on the top of your aquaeous layer in the flask will vapourise be carried
across be condensed in the condenser trickle down into your jar. It will sit atop of a bottom layer of
water.
After the last of the oil has come across, change jars leave the setup to run f aher hour, just to
make sure you got it all.
Any povidone from the pills will be stick behind in the reaction vessel.
It has been ed that some polymer that may have been left from extraction, may follow the steam.
Crystallisation :
Now we have a jar of water, with this sweet clear oil sitting on top.
Next options are to add HCl acid slowly with stirring until the oil layer disappears, then evap the whole lot
to get crystals.
Or, as I found, you may have some polymer that has come over with the steam, is now sitting in the
water layer, it looks cloudy.
I don’t want to evap all that, it will just concentrate the *censored* in there, plus its very time consuming evapping
water, plus you risk losing some meth as the water evaps.
I think you should just throw a little toluene into the jar,
then seperate.
Now your absolutly pure meth freebase is in your toluene!
Now you can either gas, f instant the now clean meth,
add minimal distillated H2O then acidify to pH 7, shake, seperate evap water f crystals.
Repeat this step if you do it this way, as some me may come in a second go.
with this process from start to finish, you shouldn’t need to re-crystalize, as your product should be the
cleanest *censored* anybody has ever seen anyway.
But you may want to, f the purpose of growing nice big crystals.
In which case, add just enough hot methanol to dissolve all your meth then place in freezer.
The secret is, the slower the evap, the bigger the crystals.
So a nice slow room temp evap over several days might be fun.
Enjoy, do attempt anything above, befe you completely underst what you are doing!
You must have a sound understing of the basics first!
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How to produce anhydrous = dry = waterfree! HCl gas using no special equipment f all your
amination steps of freebases – by Psychokitty.
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To date I have never used Strike’s Fester’s method f producing HCl gas.
Reasons f this are as follows:
1. The necessity of labaty glassware no OTC hardware.
2. what seems to be a messy proceedure using table salt but I wouldn’t know
exactly as I’ve never tried it.
3. Difficult dismantling process at least it seems to be me difficult than
mine.
I don’t remember the exact journal reference that inspired my method, but I do
know that it is described somewhere in Inganic Syntheses Vol. I.
Okay. First, here is what you need:
1. Beer bottle transparant.
2. Plastic baby syringe 15 ml capacity found at the pharmacy section at any
grocery ste.
3. Four so feet of ice-maker transparant-white polyethylene tubing found at
the hardware ste. I don’t remember the exact diameter size. All I know is
that it IS the smallest size available.
4. One table-leg stopper rubber, beige black. Aher item of which I don’t
know the size. Just take your beer bottle into the hardware ste see